Solid Phase Extraction

Solid Phase Extraction
Author: Nigel J.K. Simpson
Publsiher: CRC Press
Total Pages: 528
Release: 2000-03-15
ISBN 10: 9781420056242
ISBN 13: 1420056247
Language: EN, FR, DE, ES & NL

Solid Phase Extraction Book Review:

Demonstrating the relationship of the basic theory of solid-phase extraction (SPE) to chromatography, this comprehensive reference illustrates how SPE techniques significantly contribute to the preparation of samples for a wide variety of analytical techniques. It provides step-by-step details on the applications of SPE to environmental matrices, broad-spectrum drug screening, veterinary drug abuse, pharmaceutical drug development, biological samples, and high-throughput screening. Written by world-renowned experts in the field, the book contains helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more.

Solid Phase Extraction State of the Art and Future Perspectives

Solid Phase Extraction  State of the Art and Future Perspectives
Author: Victoria Samanidou
Publsiher: MDPI
Total Pages: 176
Release: 2019-07-11
ISBN 10: 3039211587
ISBN 13: 9783039211586
Language: EN, FR, DE, ES & NL

Solid Phase Extraction State of the Art and Future Perspectives Book Review:

This book is a collection of 13 innovative papers describing the state of the art and the future perspectives in solid-phase extraction covering several analytical fields prior to the use of gas or liquid chromatographic analysis. New sorptive materials are presented including carbon nanohorn suprastructures on paper support, melamine sponge functionalized with urea–formaldehyde co-oligomers, chiral metal–organic frameworks, UiO-66-based metal–organic frameworks, and fabric phase sorptive media for various applications. Solid-phase extraction can be applied in several formats aside from the conventional cartridges or mini-column approach, e.g., online solid-phase extraction, dispersive solid-phase microextraction, and in-syringe micro-solid-phase extraction can be very helpful for analyte pre-concentration and sample clean-up. Polycyclic musks in aqueous samples, 8-Nitroguanine in DNA by chemical derivatization antibacterial diterpenes from the roots of salvia prattii, perfluoroalkyl substances (PFASs) in aater samples by bamboo charcoal-based SPE, parabens in environmental water samples, benzotriazoles as environmental pollutants, organochlorine pesticide residues in various fruit juices and water samples and synthetic peptide purification are among the applications cited in this collection. All these outstanding contributions highlight the necessity of this analytical step, present the advantages and disadvantages of each method and focus on the green analytical chemistry guidelines that have to be fulfilled in current analytical practices.

Forensic and Clinical Applications of Solid Phase Extraction

Forensic and Clinical Applications of Solid Phase Extraction
Author: Michael J. Telepchak
Publsiher: Springer Science & Business Media
Total Pages: 370
Release: 2004-04-28
ISBN 10: 1592592929
ISBN 13: 9781592592920
Language: EN, FR, DE, ES & NL

Forensic and Clinical Applications of Solid Phase Extraction Book Review:

This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.

Handbook of Solid Phase Microextraction

Handbook of Solid Phase Microextraction
Author: Janusz Pawliszyn
Publsiher: Elsevier
Total Pages: 496
Release: 2011-11-29
ISBN 10: 0123914493
ISBN 13: 9780123914491
Language: EN, FR, DE, ES & NL

Handbook of Solid Phase Microextraction Book Review:

The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner

Solid Phase Extraction

Solid Phase Extraction
Author: Colin F. Poole
Publsiher: Elsevier
Total Pages: 740
Release: 2019-09-12
ISBN 10: 0128169079
ISBN 13: 9780128169070
Language: EN, FR, DE, ES & NL

Solid Phase Extraction Book Review:

Solid Phase Extraction thoroughly presents both new and historic techniques for dealing with solid phase extraction. It provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample. In addition, the book showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including solid-phase Microextraction, molecularly imprinted polymers, magnetic nanoparticles, and more. Written by recognized experts in their respective fields, this one-stop reference is ideal for those who need to know which technique to choose for solid phase extraction. Used in conjunction with a similar release, Liquid Phase Extraction, this book allows users to master this crucial aspect of sample preparation. Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice Includes extensive referencing that facilitates the identification of key information Aimed at both entry-level scientists and those who want to explore new techniques and methods

Liquid Phase Extraction

Liquid Phase Extraction
Author: Colin F. Poole
Publsiher: Elsevier
Total Pages: 816
Release: 2019-08-29
ISBN 10: 0128169125
ISBN 13: 9780128169124
Language: EN, FR, DE, ES & NL

Liquid Phase Extraction Book Review:

Liquid Phase Extraction thoroughly presents both existing and new techniques in liquid phase extraction. It not only provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample, but also showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including countercurrent chromatography, pressurized-liquid extraction, single-drop Microextraction, and more. Written by recognized experts in their respective fields, it serves as a one-stop reference for those who need to know which technique to choose for liquid phase extraction. Used in conjunction with a similar release, Solid Phase Extraction, it allows users to master this crucial aspect of sample preparation. Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice Includes extensive referencing that facilitates the identification of key information Aimed at both entry-level scientists and those who want to explore new techniques and methods

Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis

Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis
Author: Jussi Meriluoto,Lisa Spoof,Geoffrey A. Codd
Publsiher: John Wiley & Sons
Total Pages: 576
Release: 2017-01-30
ISBN 10: 1119068681
ISBN 13: 9781119068686
Language: EN, FR, DE, ES & NL

Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis Book Review:

A valuable handbook containing reviews, practical methods and standard operating procedures. A valuable and practical working handbook containing introductory and specialist content that tackles a major and growing field of environmental, microbiological and ecotoxicological monitoring and analysis Includes introductory reviews, practical analytical chapters and a comprehensive listing of almost thirty Standard Operating Procedures (SOPs) For use in the laboratory, in academic and government institutions and industrial settings

Applications of Metal Organic Frameworks and Their Derived Materials

Applications of Metal Organic Frameworks and Their Derived Materials
Author: Inamuddin,Rajender Boddula,Mohd Imran Ahamed,Abdullah M. Asiri
Publsiher: John Wiley & Sons
Total Pages: 496
Release: 2020-05-04
ISBN 10: 111965095X
ISBN 13: 9781119650959
Language: EN, FR, DE, ES & NL

Applications of Metal Organic Frameworks and Their Derived Materials Book Review:

Metal–organic frameworks (MOFs) are porous crystalline polymers constructed by metal sites and organic building blocks. Since the discovery of MOFs in the 1990s, they have received tremendous research attention for various applications due to their high surface area, controllable morphology, tunable chemical properties, and multifunctionalities, including MOFs as precursors and self-sacrificing templates for synthesizing metal oxides, heteroatom-doped carbons, metal-atoms encapsulated carbons, and others. Thus, awareness and knowledge about MOFs and their derived nanomaterials with conceptual understanding are essential for the advanced material community. This breakthrough new volume aims to explore down-to-earth applications in fields such as biomedical, environmental, energy, and electronics. This book provides an overview of the structural and fundamental properties, synthesis strategies, and versatile applications of MOFs and their derived nanomaterials. It gives an updated and comprehensive account of the research in the field of MOFs and their derived nanomaterials. Whether as a reference for industry professionals and nanotechnologists or for use in the classroom for graduate and postgraduate students, faculty members, and research and development specialists working in the area of inorganic chemistry, materials science, and chemical engineering, this is a must-have for any library.

Sample Preparation in LC MS Bioanalysis

Sample Preparation in LC MS Bioanalysis
Author: Wenkui Li,Wenying Jian,Yunlin Fu
Publsiher: John Wiley & Sons
Total Pages: 384
Release: 2019-03-12
ISBN 10: 111927429X
ISBN 13: 9781119274292
Language: EN, FR, DE, ES & NL

Sample Preparation in LC MS Bioanalysis Book Review:

Revised and Expanded Handbook Provides Comprehensive Introduction and Complete Instruction for Sample Preparation in Vital Category of Bioanalysis Following in the footsteps of the previously published Handbook of LC-MS Bioanalysis, this book is a thorough and timely guide to all important sample preparation techniques used for quantitative Liquid Chromatography–Mass Spectrometry (LC-MS) bioanalysis of small and large molecules. LC-MS bioanalysis is a key element of pharmaceutical research and development, post-approval therapeutic drug monitoring, and many other studies used in human healthcare. While advances are continually being made in key aspects of LC-MS bioanalysis such as sensitivity and throughput, the value of research/study mentioned above is still heavily dependent on the availability of high-quality data, for which sample preparation plays the critical role. Thus, this text provides researchers in industry, academia, and regulatory agencies with detailed sample preparation techniques and step-by-step protocols on proper extraction of various analyte(s) of interest from biological samples for LC-MS quantification, in accordance with current health authority regulations and industry best practices. The three sections of the book with a total of 26 chapters cover topics that include: Current basic sample preparation techniques (e.g., protein precipitation, liquid-liquid extraction, solid-phase extraction, salting-out assisted liquid-liquid extraction, ultracentrifugation and ultrafiltration, microsampling, sample extraction via electromembranes) Sample preparation techniques for uncommon biological matrices (e.g., tissues, hair, skin, nails, bones, mononuclear cells, cerebrospinal fluid, aqueous humor) Crucial aspects of LC-MS bioanalytical method development (e.g., pre-analytical considerations, derivation strategies, stability, non-specific binding) in addition to sample preparation techniques for challenging molecules (e.g., lipids, peptides, proteins, oligonucleotides, antibody-drug conjugates) Sample Preparation in LC-MS Bioanalysis will prove a practical and highly valuable addition to the reference shelves of scientists and related professionals in a variety of fields, including pharmaceutical and biomedical research, mass spectrometry, and analytical chemistry, as well as practitioners in clinical pharmacology, toxicology, and therapeutic drug monitoring.

Handbook of Pharmaceutical Analysis by HPLC

Handbook of Pharmaceutical Analysis by HPLC
Author: Satinder Ahuja,Michael Dong
Publsiher: Elsevier
Total Pages: 600
Release: 2005-02-09
ISBN 10: 9780080455181
ISBN 13: 0080455182
Language: EN, FR, DE, ES & NL

Handbook of Pharmaceutical Analysis by HPLC Book Review:

High pressure liquid chromatography–frequently called high performance liquid chromatography (HPLC or, LC) is the premier analytical technique in pharmaceutical analysis and is predominantly used in the pharmaceutical industry. Written by selected experts in their respective fields, the Handbook of Pharmaceutical Analysis by HPLC Volume 6, provides a complete yet concise reference guide for utilizing the versatility of HPLC in drug development and quality control. Highlighting novel approaches in HPLC and the latest developments in hyphenated techniques, the book captures the essence of major pharmaceutical applications (assays, stability testing, impurity testing, dissolution testing, cleaning validation, high-throughput screening). A complete reference guide to HPLC Describes best practices in HPLC and offers 'tricks of the trade' in HPLC operation and method development Reviews key HPLC pharmaceutical applications and highlights currents trends in HPLC ancillary techniques, sample preparations, and data handling

Solid Phase Microextraction

Solid Phase Microextraction
Author: Gangfeng Ouyang,Ruifen Jiang
Publsiher: Springer
Total Pages: 308
Release: 2016-11-24
ISBN 10: 366253598X
ISBN 13: 9783662535981
Language: EN, FR, DE, ES & NL

Solid Phase Microextraction Book Review:

This book offers comprehensive information on the developments and applications of the solid phase microextraction (SPME) technique. The first part of the book briefly introduces readers to the fundamentals of SPME, while subsequent sections describe the applications of SPME technique in detail, including environmental analysis (air, water, soil/sediments), food analysis (volatile/nonvolatile compounds), and bioanalysis (plants, animal tissues, body fluids). The advantages and future challenges of the SPME technique are also discussed. Including recent research advances and further developments of SPME, the book offers a practical reference guide and a valuable resource for researchers and users of SPME techniques. The target audience includes analytical chemists, environmental scientists, biological scientists, material scientists, and analysts, as well as students at universities/institutes in related fields. Dr. Gangfeng Ouyang is a Professor at the School of Chemistry and Chemical Engineering, Sun Yat-sen University, China. Dr. Ruifen Jiang is an Associate Professor at the School of Environment, Jinan University, China.

Critical and Rare Earth Elements

Critical and Rare Earth Elements
Author: Abhilash,Ata Akcil
Publsiher: CRC Press
Total Pages: 384
Release: 2019-11-11
ISBN 10: 0429659814
ISBN 13: 9780429659812
Language: EN, FR, DE, ES & NL

Critical and Rare Earth Elements Book Review:

This book is aimed to compile the distribution of rare earth elements in various resources with their processing from secondary resources. It includes details of various processes developed for extraction of rare earth elements from varied raw materials ranging from e-wastes, tailings, process wastes and residues. It emphasizes importance of processing of the secondary resources to assist environmental remediation of such untreated wastes and get finished products. It covers all aspects of rare metals and rare earth metals in one volume covering extraction, separation and recycling of secondary resources for extraction of these metals along with relevant case studies.

Analytical Microextraction Techniques

Analytical Microextraction Techniques
Author: M. Valcárcel,S. Cárdenas,R. Lucena
Publsiher: Bentham Science Publishers
Total Pages: 425
Release: 2017-01-13
ISBN 10: 1681083795
ISBN 13: 9781681083797
Language: EN, FR, DE, ES & NL

Analytical Microextraction Techniques Book Review:

Sample treatment has been the focus of intensive research in the last 20 years since it still remains a bottleneck in precise analytical procedures. The low concentration of the target analytes, the large amount of potential interfering agents and the incompatibility of the sample matrix with the instrumental techniques are the main reasons for these bottlenecks. In most of these methods, sample treatment is an unavoidable step and it has a clear influence on the quality (sensitivity, selectivity, and accuracy) of the final analytical results. While the usefulness of microextraction techniques has been established, their complete acceptance in analytical laboratories (including official methods of analysis) depends on their successful automation and integration with conventional analytical instrumentation. Analytical Microextraction Techniques presents comprehensive information about several analytical methods that are useful in the laboratory. These include: sorptive microextraction, solid and liquid phase microextraction, packed sorbent microextraction, miniaturized dispersive solid-phase extraction, thin film and nanoparticle based techniques, and membrane-based techniques. This is a vital reference on microextraction and sample preparation techniques for applied chemistry students, analytical chemists and laboratory technicians.

Sample Preparation Techniques in Analytical Chemistry

Sample Preparation Techniques in Analytical Chemistry
Author: Somenath Mitra
Publsiher: John Wiley & Sons
Total Pages: 488
Release: 2004-04-07
ISBN 10: 9780471457824
ISBN 13: 0471457825
Language: EN, FR, DE, ES & NL

Sample Preparation Techniques in Analytical Chemistry Book Review:

The importance of accurate sample preparation techniques cannot be overstated--meticulous sample preparation is essential. Often overlooked, it is the midway point where the analytes from the sample matrix are transformed so they are suitable for analysis. Even the best analytical techniques cannot rectify problems generated by sloppy sample pretreatment. Devoted entirely to teaching and reinforcing these necessary pretreatment steps, Sample Preparation Techniques in Analytical Chemistry addresses diverse aspects of this important measurement step. These include: * State-of-the-art extraction techniques for organic and inorganic analytes * Sample preparation in biological measurements * Sample pretreatment in microscopy * Surface enhancement as a sample preparation tool in Raman and IR spectroscopy * Sample concentration and clean-up methods * Quality control steps Designed to serve as a text in an undergraduate or graduate level curriculum, Sample Preparation Techniques in Analytical Chemistry also provides an invaluable reference tool for analytical chemists in the chemical, biological, pharmaceutical, environmental, and materials sciences.

Analytical Solid Phase Extraction

Analytical Solid Phase Extraction
Author: James S. Fritz,James Sherwood Fritz
Publsiher: Wiley-VCH
Total Pages: 209
Release: 1999-06-25
ISBN 10:
ISBN 13: UOM:39015047451466
Language: EN, FR, DE, ES & NL

Analytical Solid Phase Extraction Book Review:

New trends in solid-phase extraction for analytical use--a practical introduction. Owing to its low cost, ease of use, and nonpolluting means of preparing samples for analysis, solid-phase extraction (SPE) is fast overtaking traditional liquid--liquid methods in clinical, pharmaceutical, agricultural, and industrial applications. This book describes what analytical scientists and technicians need to know about this emerging procedure: how it works, how to choose from available techniques, how to utilize it effectively in the laboratory. Along with the historical perspective and fundamental principles, this practical book reviews the latest literature on solid-phase materials, equipment, and applications--including EPA-endorsed techniques. Special features include: * Coverage of separation and uptake methods. * Promising developments in the use of membrane disks. * The advantages of using polymeric resins over silica materials. * Mechanism and use of ion-exchange materials for SPE. * A remarkably complete chapter on the extraction of metal ions. * Groundbreaking research in the miniaturized SPE technique. Readers seeking additional information on SPE procedures may wish to consult: SOLID-PHASE EXTRACTION, Principles and Practice, E. M. Thurman and M. S. Mills 1998 (0-471-61422-X) 384 pp. SOLID-PHASE MICROEXTRACTION Theory and Practice Janusz Pawliszyn 1997 (0-471-19034-9) 264 pp.

Beginner s Guide to SPE

Beginner s Guide to SPE
Author: Waters Corporation
Publsiher: Waters Corporation
Total Pages: 212
Release: 2014-04-21
ISBN 10: 9781467539203
ISBN 13: 1467539201
Language: EN, FR, DE, ES & NL

Beginner s Guide to SPE Book Review:

Through over 150 full color diagrams and straight forward text, readers will understand the power and usefulness of solid-phase extraction and how it helps solve sample preparation challenges. This 212 page book covers many topics including SPE device formats, sorbent considerations, mobile phase selection, and troubleshooting. A must read for anyone starting out in analytical chromatography as well as seasoned chemists looking to add solid-phase extraction to their skills set. Looking for something else? Learn a new technique or technology with the Waters Primers Series, view other titles available here: http://www.wiley.com/go/waters

Modern Sample Preparation for Chromatography

Modern Sample Preparation for Chromatography
Author: Serban C. Moldoveanu,Victor David
Publsiher: Elsevier
Total Pages: 453
Release: 2014-10-18
ISBN 10: 0444543228
ISBN 13: 9780444543226
Language: EN, FR, DE, ES & NL

Modern Sample Preparation for Chromatography Book Review:

Sample preparation is applied to make real world samples amenable for chromatographic analysis, or to improve the results of this type of analysis. A wide variety of procedures are applied for this purpose, and their description is the main goal of the present book. The principles of these procedures are explained, discussing their advantages and disadvantages, and their applicability to different types of samples as well as their fit for different types of chromatographic analysis. This provides a guide for choosing the appropriate sample preparation for a given analysis. The book also contains numerous literature references and examples of sample preparation for different matrices. The material is presented in three parts, one discussing physical methods used in sample preparation such as filtration, distillation, solvent extraction, solid phase extraction, electro-separations. Presents in a systematic way numerous techniques applied for sample preparation for chromatographic analysis Provides an up to date source of information regarding the progress made in sample preparation for chromatography Describes examples for specific type of matrices, providing a guide for choosing the appropriate sample preparation method for a given analysis

Miniaturization in Sample Preparation

Miniaturization in Sample Preparation
Author: Francisco Pena Pereira
Publsiher: Walter de Gruyter GmbH & Co KG
Total Pages: 463
Release: 2014-01-01
ISBN 10: 3110427265
ISBN 13: 9783110427264
Language: EN, FR, DE, ES & NL

Miniaturization in Sample Preparation Book Review:

Miniaturization is a challenge thrown down to analytical chemistry. The replacement of conventional analytical systems by miniaturized alternatives during the last years is noticeable. Specifically, the miniaturization of traditional sample preparation techniques (e.g., solid-phase extraction or solvent extraction) led to the development of environmentally benign analytical methods. This book aims to provide an overview of the challenges and achievements inthe application of the miniaturized sample preparation methods in analytical laboratories. It includes both theoretical and practical aspects of miniaturized sample preparation approaches and hence should be of interest to researchers, students and teachers of analytical and bioanalytical chemistry, environmental sciences and environmental engineering.

Solid Phase Microextraction

Solid Phase Microextraction
Author: Constantinos K. Zacharis,Paraskevas D. Tzanavaras
Publsiher: MDPI
Total Pages: 266
Release: 2020-02-07
ISBN 10: 303928262X
ISBN 13: 9783039282623
Language: EN, FR, DE, ES & NL

Solid Phase Microextraction Book Review:

This book covers the most recent research activities and achievements regarding to the solid phase microextraction (SPME) technique. It is a powerful sample preparation tool that addresses the new challenges of analytical laboratories. Among others, its fundamental applications involved the sampling of volatile compounds from various matrixes. The demonstrated topics ranged from aroma characterization of various fruits, essential oils to the utilization of SPME for in-tube extraction and isolation of selected compounds from complex samples followed by state-of-the-art analytical techniques.

Extraction Techniques in Analytical Sciences

Extraction Techniques in Analytical Sciences
Author: John R. Dean
Publsiher: John Wiley & Sons
Total Pages: 308
Release: 2010-05-18
ISBN 10: 9780470682500
ISBN 13: 0470682507
Language: EN, FR, DE, ES & NL

Extraction Techniques in Analytical Sciences Book Review:

This book coves one of the most important areas in analytical sciences, extraction techniques for organic compounds in environmental and related matrices. This text discusses all of the key stages for analysing a sample for organic compounds from the initial sampling protocols, the range of different extraction techniques for solid, liquid and air samples through to the final chromatographic analysis. The topics covered include: Initial steps for solid, aqueous and air sampling. Extraction techniques for aqueous samples, including LLE, purge and trap, SPE, SPME, SBSE, SDME, membrane microextraction and MPES. Extraction techniques for solid samples, including Soxhlet, 'Soxtec', Shake-flask, sonication, PFE, MAE, SFE and MSPD. Extraction techniques for air sampling, including whole air, enrichment approaches and desorption techniques. Pre-concentration approaches for post-extraction. Practical aspects for chromatographic analysis (GC and HPLC) of organic compounds. Quality assurance aspects of analysis. Health and safety considerations. Key features include: Up-to-date information on the latest development in extraction techniques for organic compounds in environmental and food matrices. Ideal for use as a self-study guide, as the basis of a taught course or guided reading for new 'early-career' researchers. Includes a guide for the reader to other sources of information. Extraction Techniques in Analytical Sciences is suitable for undergraduate and postgraduate students, as well as providing an invaluable starting point for individuals undertaking applied research in the fields of analytical, bioanalytical, environmental and food sciences. The Analytical Techniques in the Sciences series of books provides coverage of all of the major analytical techniques and their application in the most important areas of physical, life and materials science. Each text is presented in an open learning/distance learning style, in which the learning objectives are clearly identified. the reader's understanding of the material is constantly evaluated by the use of self-assessment and discussion questions.